AuCu纳米薄膜中孪晶-位错相互作用的原子尺度观察

冯元元,王占鑫,马 琰,张 旭,杨成鹏*,王立华*,韩晓东

AuCu纳米薄膜中孪晶-位错相互作用的原子尺度观察

冯元元,王占鑫,马  琰,张  旭,杨成鹏*,王立华*,韩晓东

(1. 北京工业大学固体微结构与性能研究所,北京市先进材料微结构与性能重点实验室,北京 100124;2. 中国科学院苏州纳米技术与纳米仿生研究所,江苏 苏州 215123;3. 南方科技大学材料科学与工程系,广东 深圳 518000)

摘 要  本文利用原位实验技术,在透射电镜中对AuCu合金纳米薄膜中的孪晶与位错相互作用行为进行了原子尺度观察。原位原子尺度实验研究发现了多种位错-孪晶相互作用行为,即偏位错交叉滑移诱导孪晶增厚行为、全位错穿越孪晶界行为,以及全位错在孪晶界分解重组诱导退孪晶行为。本实验为理解纳米合金材料中孪晶-位错反应机理提供了原位原子尺度证据,对利用缺陷相互作用提高纳米合金材料的强韧性具有一定借鉴意义。

关键词  纳米晶薄膜;塑性变形;位错;孪晶

中图分类号:O733; TG115. 5+2; TG115. 21+5. 3    

文献标识码:A Doi:10.3969/j.issn.1000-6281.2025.06.002

 

Atomic-scale observation of twin-dislocation interactions in AuCu nanofilms

FENG Yuanyuan1, WANG Zhanxin1, MA Yan1, ZHANG Xu1, YANG Chengpeng12*, WANG Lihua1*, HAN Xiaodong13

(1. Beijing Key Lab of Microstructure and Property of Advanced Material, Institute of Microstructure and Properties of Advanced Materials, Beijing University of Technology, Beijing 100124; 2. Suzhou Institute of Nano-Tech and Nano-Bionics, Chinese Academy of Sciences, Suzhou Jiangsu 215123;Department of Materials Science and Engineering, Nanfang University of Science and Technology, Shenzhen Guangdong 518000,China)

Abstract  In this study, atomic-scale observations of twin-dislocation interactions in AuCu alloy nanofilms were conducted using in situ transmission electron microscopy. The in-situ experiments revealed various interaction behaviors dislocations and twins, including biased dislocation cross-slip induced twin thickening, transmission of full dislocations across twin boundaries, and dissociation and recombination of full dislocations leading to detwinning. These observations provide direct atomic-scale evidence for understanding the mechanisms of twin-dislocation reactions in nano-alloyed materials, offering valuable insights for optimzing defect interactions to improve the strength and toughness of nano-alloyed materials.

Keywords  nanocrystalline thin films; plastic deformation; dislocations; twins