形变时效对Al-2.4Cu-0.9Li-0.7Mg合金的显微组织和力学性能的影响
邹富强,李石勇,伍翠兰*,巩向鹏,罗世芳,周 琳
(湖南大学材料科学与工程学院高分辨电镜中心,湖南 长沙 410082)
摘 要 本文采用透射电镜观察、硬度测试和拉伸性能测试等手段,研究了形变时效对Al-2.4Cu-0.9Li-0.7Mg (wt.%)合金的显微组织和力学性能的影响。结果表明:固溶后直接150~180℃时效的T6试样主要析出相为高密度弥散分布的GPB区和少量的S相、T1相。时效前引入预变形的T8工艺可显著提高合金的强度但塑性大幅降低,T8试样中主要析出相为S相和T1相;相对T6工艺,T8工艺析出的S相和T1相尺寸减小,但由于其易于在位错胞或亚晶界上形核长大,因此析出相分布不均匀。在预变形前引入预时效的TMT工艺不仅提高合金的强度且塑性得到改善,其主要原因是,TMT工艺使得合金基体内S相与T1相数量密度增加、尺寸更细小、分布更均匀。
关键词 形变时效;析出相;强度;塑性;TEM表征
中图分类号:TG156.9;TG113;TG155.1;TG115.21+5.3 文献标识码:A doi:10.3969/j.issn.1000-6281.2019.06.007
Effect of thermo-mechanical treatment on the microstructure and mechanical properties of Al-2.4Cu-0.9Li-0.7Mg alloy
ZOU Fu-qiang,LI Shi-yong,WU Cui-lan*,GONG Xiang-peng,LUO Shi-fang,ZHOU Lin
(College of Material Science and Engineering of Hunan University,Changsha Hunan 410082, China)
Abstract Effect of thermo-mechanical treatment on the microstructure and mechanical properties of Al-2.4Cu-0.9Li-0.7Mg (wt.%) alloy were investigated by means of transmission electron microscopy, hardness test and tensile test. The results show that after solution treatment followed by ageing at 150~180℃, the main precipitates of T6 samples are high density dispersed GPB zone, a few S and T1 phases. The T8 process, which involves large pre-deformation and aging, can significantly improve the strength of the alloy, but decrease the plasticity. The main precipitates of T8 samples are S phase and T1 phase. Compared with T6 samples, the size of S phase and T1phase precipitating during T8 process is smaller. However, the distribution of S precipitates and T1 precipitates is heterogeneous because these precipitates tend to nuclear and grow along the dislocation cell or sub-grain boundary. Compared with the T8 process, TMT process introducing pre-aging before pre-deformation not only improves the strength of alloy, but also improves the plasticity. The main reason is that the TMT process increases the number density of S phase and T1 phase, reduces the size of precipitates and makes the precipitates to distribute more uniformly in the alloy matrix.
Keywords thermo-mechanical treatment;precipitate;strength;plasticity;TEMcharacterize
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